Patent · US Expired

Recovery of alumina values from alunite ore

US4618480A · kind A · utility

2Cited by
11References
37Claims
0Family size

Assignee

Inventors

Key dates

Filing dateAug 15, 1984
Grant dateOct 21, 1986
Priority date
Expiry dateAug 15, 2004

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01F7/47
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

A novel process for the recovery of alumina and potassium sulfate from alunite is provided comprising leaching the alunite with potassium hydroxide to which no sodium materials have been added, said leach solution being saturated with potassium sulfate. Aluminum values are solubilized into the leachate, and potassium and sulfur values are rendered soluble, but remain in the residue. The leachate is desilicated if necessary, preferably with lime, and aluminum trihydroxide is precipitated therefrom, followed by calcining to alumina product. The residue is leached to solubilize potassium sulfate in a secondary leach and the potassium sulfate product crystallized therefrom. Potassium hydroxide is regenerated from a portion of the potassium sulfate secondary leachate by several methods. Novel procedures for regenerating alkali metal hydroxides from the corresponding sulfates are also provided including routes involving formates and carbonates as intermediates and pyrohydrolysis.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.