Process for the preparation of 2,6-dichlorobenzoxazole
US4658034A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Feb 21, 1985 |
| Grant date | Apr 14, 1987 |
| Priority date | — |
| Expiry date | Feb 21, 2005 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D263/58
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
A process for the preparation of 2,6-dichlorobenzoxazole, which comprises reacting 6-chlorobenzoxazolone in the presence of chlorine, phosphorus trichloride and phosphoryl chloride, or in mixtures of phosphorus pentachloride and phosphoryl chloride, at temperatures of 150.degree. to 170.degree. C., under pressure, the weight ratio of chlorine and phosphorus trichloride to phosphoryl chloride or of phosphorus pentachloride to phosphoryl chloride being 0.15:1 to 0.60:1.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.