Process for the production of a spray-dried nonionic washing aid

US4661281A · kind A · utility

Assignee

• Henkel Kommanditgesellschaft auf Aktien · DE

Inventors

• Wolfgang Seiter · Neuss, DE
• Ingo Wegener · Goldkronach, DE
• Herbert Reuter · Hilden, DE

Key dates

• Filing date: Jun 28, 1985
• Grant date: Apr 28, 1987
• Expiry date: Jun 28, 2005

Classification

• Technology area (CPC C): Chemistry; Metallurgy
• CPC primary: C11D3/128
• WIPO field: Basic materials chemistry
• WIPO sector: Chemistry

Abstract

A free-flowing washing powder of low specific gravity (powder density 300 to 500 g/l) and containing large quantities of nonionic surfactants is produced by spray-drying an aqueous suspension containing on the spray-dried basis (A) from 15 to 30% by weight of nonionic tensides, (B) from 8 to 18% by weight of sodium silicate, (C) from 25 to 55% by weight of finely crystalline zeolite, (D) from 0 to 25% by weight of sodium tripolyphosphate, (E) no more than 3% by weight of soap and synthetic anionic tensides, and from 35 to 50% by weight of water. The suspension, which has a temperature of from 75.degree. C. to 90.degree. C., is sprayed through nozzles into a drying zone under a pressure of from 35 to 100 bar. The drying gas flowing in countercurrent has an entry temperature of from 160.degree. C. to 240.degree. C. and an exit temperature of from 80.degree. C. to 95.degree. C. The spray-dried product contains from 9 to 16% by weight of water which is removable at a drying temperature of 130.degree. C.