Patent · US Expired

Process for the preparation of compounds containing a difluoromethylene or trifluoromethyl group

US4668830A · kind A · utility

9Cited by
3References
15Claims
0Family size

Assignee

Inventor

Key dates

Filing dateDec 17, 1985
Grant dateMay 26, 1987
Priority date
Expiry dateDec 17, 2005

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C41/50
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A process for the preparation of compounds containing a difluoromethylene or trifluoromethyl group. A compound containing a carbonyl group, preferbly an acid, acid halide, amide, ketone or any compound containing a perhaloalkylcarbonyl moiety is placed, in anhydrous liquid hydrofluoric acid, in contact with boron trifluoride in a quantity such that the absolute pressure of boron trifluoride in the reaction system is at least one bar for a time sufficient to convert the carbonyl group to a difluormethylene or trifluoromethyl group. The compounds obtained are useful as synthesis intermediates in the pharmaceutical, plant-protection and dye industries, as anesthetics or as heat-transfer and lubricating fluids.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.