Process for the preparation of 2-arylamino-4,6-dichloro-s-triazines
US4683308A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jan 21, 1986 |
| Grant date | Jul 28, 1987 |
| Priority date | — |
| Expiry date | Jan 21, 2006 |
Classification
- Technology area (CPC D)Textiles; Paper
- CPC primaryD06M13/313
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
In the preparation of a 2-arylamino-4,6-dichloro-s-triazine of the formula ##STR1## in which R.sup.1 is an optionally substituted aryl radical, and PA0 R.sup.2 is hydrogen or alkyl, by reacting cyanuric chloride of the formula ##STR2## with a virtually water-insoluble arylamine of the formula ##STR3## at a temperature between 0.degree. and 100.degree. C., the improvement which comprises effecting the reaction in water at an acid pH in the presence of a virtually water-insoluble organic solvent. The resulting aqueous phase contains the triazine in such high purity and concentration that it can be used without further purification. The organic solvent can be recycled.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.