Polyalkylene polyamines via vapor phase reaction using inert gas
US4720588A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jan 16, 1986 |
| Grant date | Jan 19, 1988 |
| Priority date | — |
| Expiry date | Jan 16, 2006 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C209/16
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
This invention pertains to an improved process for preparing noncyclic polyalkylene polyamine compounds in high selectivity by reacting an alkanolamine and an alkylene amine in the presence of an inert gas and an acidic catalyst. The improvement resides in effecting the reaction under fixed bed catalytic conditions and maintaining the reaction conditions such that a vapor phase condition exists for the reaction mixture comprising both reactants and products. To accomplish the formation of vapor phase conditions sufficient inert gas is injected into the feedstream along with alkanolamine and alkylene amine so that the dew point temperature of the reaction product mix is below the reaction temperature at reaction pressure.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.