Patent · US Expired

Chemical milling method for interiors of narrow tubes

US4726878A · kind A · utility

1Cited by
3References
5Claims
0Family size

Assignee

Inventor

Key dates

Filing dateDec 8, 1986
Grant dateFeb 23, 1988
Priority date
Expiry dateDec 8, 2006

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC23F1/02
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

A method for etching patterns on the interior surface of narrow metal tubes. A thin tube having a narrow internal diameter is dipped into a maskant solution to a depth equal to the distance from the tube end etching is to be stopped. A thixotropic maskant having high edge thickness along the dipped edge is required. The shaft is removed from the maskant and dried. Plural dips to increase maskant thickness may be used, if desired. Both ends of the tube may be dipped to localize the area to be etched away from both ends. The tube is placed in an etching solution which is agitated and replenished as desired. After a suitable period, the tube is removed from the etchant, rinsed, dried and the maskant peeled away. A sharp, even, etched edge results, with a smooth fillet and no leaks of etchant through the maskant. The quality of the etch will be greatly increased where an iron-nickel-chromium alloy such as 718 Inconel is being etched by maintaining the metal ion ratio of the etchant at from about 50 to 60 g/l for the iron ion and from about 35 to 49 g/l for the nickel ion, with the grams per liter of the nickel ion always less than the iron ion.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.