Patent · US Expired

Continuous process for the production of aqueous polyurethane-urea dispersions

US4742095A · kind A · utility

32Cited by
11References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 21, 1986
Grant dateMay 3, 1988
Priority date
Expiry dateOct 21, 2006

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC08G18/5042
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

The present invention is directed to a continuous process for the production of aqueous polyurethane-urea dispersions by PA0 (a) mixing an emulsifiable isocyanate-terminated prepolymer with an aqueous medium in a low shear, stator-rotor dynamic mixer operating at a speed of about 500 to 8000 rpm utilizing a mixing wattage of about 0.3 to 10.0 watts/cubic centimeter and a mixing volume of at least about 0.1 liters, the average residence time of the aqueous medium and the prepolymer being about 1 to 30 seconds and the overall flow rate through the dynamic mixer being at least about 50 kg/h and PA0 (b) reacting the dispersed isocyanate-terminated prepolymer prepared in (a) with a polyamine chain extender to form an aqueous polyurethane-urea dispersion.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.