Patent · US Expired

Process for producing a clean hydrocarbon fuel from high calcium coal

US4753033A · kind A · utility

16Cited by
58References
28Claims
0Family size

Assignee

Inventor

Key dates

Filing dateFeb 5, 1987
Grant dateJun 28, 1988
Priority date
Expiry dateFeb 5, 2007

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC10L9/02
  • WIPO fieldBasic materials chemistry
  • WIPO sectorChemistry

Abstract

A process for substantially reducing the amount of insoluble fluoride-forming species in a coal feed material comprising slurrying a coal feed with a fluoride acid in the presence of an amount of fluoride-complexing species at least equal to the amount necessary to form tightly-bound complex ions with substantially all free-fluoride-ions in the slurry to produce a leached coal product and a spent leach liquor, and separating the leached coal product from the spent leach liquor. The process produces a clean purified fuel with ash content of less than about 5%, and preferably less than about 1%. Loss of fluorine values by formation of insoluble fluorides is minimized. Alkali metals and alkaline earths are substantially dissolved. The process generally comprises sizing the coal to 10 mm or less, leaching the sized coal with hydrofluoric acid in the presence of a determinable amount of a fluoride-complexing species such as silicon or aluminum, separating the leached coal from the spent leach liquor, and optionally some or all of the following: (a) pre-drying or physically beneficiating feed with high moisture or high mineral matter (ash) content; (b) cleaning the leached coal by washin…

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.