Preparation of anhydrous aluminum chloride
US4769227A · kind A · utility
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4Claims
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Key dates
| Filing date | May 28, 1987 |
| Grant date | Sep 6, 1988 |
| Priority date | — |
| Expiry date | May 28, 2007 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC01P2002/72
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
Anhydrous aluminum chloride is prepared by reacting .gamma.-alumina with carbon monoxide and chlorine and/or phosgene in a fluidized bed at from 400.degree. to 700.degree. C. The .gamma.-alumina used gives, with CuK.sub..alpha. radiation, an X-ray diffraction pattern whose intensity at the diffraction angle 2.sup..crclbar. =42.8.degree..+-.0.4.degree. divided by the intensity at the diffraction angle 2.sup..crclbar. =45.7.degree..+-.0.2.degree. is .ltoreq.0.38.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.