Patent · US Expired

Hydrothermal process for preparing zirconia-alumina base ultra-fine powders of high purity

US4769351A · kind A · utility

14Cited by
3References
8Claims
0Family size

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Key dates

Filing dateMay 4, 1987
Grant dateSep 6, 1988
Priority date
Expiry dateMay 4, 2007

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S977/90
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

A process for preparing a zirconia-alumina base composite ultra-fine powder is described, including the steps of: mixing an aluminum salt or an alumina hydrate with an aqueous zirconium oxychloride solution, with or without metal salt acting as a stabilizer; mixing urea or a substance capable of generating ammonia by hydrolysis with the resulting mixture; and allowing the mixture to react at a temperature of 140.degree. to 300.degree. C. and a pressure of 4 to 150 kg/cm.sup.2 in a high-temperature and -pressure vessel. The reaction product is further dried, calcined and crushed to obtain an ultra-fine powder.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.