Patent · US Expired

Method of preparation of a combined ZSM-5-ferrierite aluminosilicate

US4797266A · kind A · utility

9Cited by
10References
7Claims
0Family size

Assignee

Inventor

Key dates

Filing dateAug 7, 1986
Grant dateJan 10, 1989
Priority date
Expiry dateAug 7, 2006

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S423/23
  • WIPO fieldBasic materials chemistry
  • WIPO sectorChemistry

Abstract

A method of preparation of a combined ZSM-5 and ferrierite aluminosilicate is disclosed utilizing a crystallization admixture comprising sodium silicate, a compound of aluminum, sodium oxide, water and a combination of amines comprising piperidine and an aliphatic amine selected from the group of n-butylamine and tetrapropylammonium hydroxide. The latter chosen amine is directive for a ZSM-5 aluminosilicate while the former is directive for a ferrierite aluminosilicate. Examination by Scanning Electron Microscope (SEM) demonstrates a different catalyst morphology than a catalyst synthesized using silica gel and pyridine. The resultant catalyst is useful in the dewaxing of lubricating oils, especially those oils not necessarily treatable by a unitary ferrierite or a unitary ZSM-5 catalyst.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.