Patent · US Expired

Process for preparation of synthetic mordenite molded body

US4861571A · kind A · utility

13Cited by
4References
12Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 19, 1986
Grant dateAug 29, 1989
Priority date
Expiry dateSep 19, 2006

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01B33/2861
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

A synthetic mordenite molded body is prepared by a process wherein a starting mixture comprising, as the main components, a silica source, an alumina source, an alkali source and water is molded into a starting molded body, the molded body is calcined and the calcined molded body is heated in an aqueous solution of sodium silicate. The starting mixture has incorporated therein a mordenite seed crystal powder. When the molded body is calcined, the temperature is elevated by heating to a calcination temperature not lower than 400.degree. C. at an average rate of at least 10.degree. C./min and calcination is conducted at the calcination temperature within a time period of 2 hours. When the calcined molded body is crystallized, an aqueous solution of sodium silicate having an SiO.sub.2 concentration of 7 to 25% by weight, an Na.sub.2 O concentration of 2 to 8% by weight and an SiO.sub.2 /Na.sub.2 O molar ratio of from 0.9 to 4.0 is used as the aqueous solution of sodium silicate.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.