Synthesis of crystalline SAPO-37
US4898722A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Dec 19, 1984 |
| Grant date | Feb 6, 1990 |
| Priority date | — |
| Expiry date | Dec 19, 2004 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S423/30
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
An improved method for synthesis of improved silicoaluminophosphate SAPO-37 is provided. The method comprises (1) preparing a two-phase reaction mixture containing particular components and comprising both a liquid organic phase and a liquid aqueous phase; (2) heating the reaction mixture at a rate of from 5.degree. C. to 200.degree. C. per hour to a temperature of from 80.degree. C. to 200.degree. C.; agitating the reaction mixture in a manner sufficient to intimately admix said liquid organic and aqueous phases with each other; (4) once nucleation of the silicoaluminophosphate occurs, heating the agitated reaction mixture at rate of from 5.degree. C. to 200.degree. C. per hour to a temperature of from 100.degree. C. to 300.degree. C.; (5) maintaining the agitated reaction mixture at a temperature of from 100.degree. C. to 300.degree. C. and a pH of from 2 to 9 until crystals of the desired silicoaluminophosphate are formed; and (6) recovering silicoaluminophosphate material from the reaction mixture.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.