Catalyst preparation using supercritical solvent
US4916108A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Aug 25, 1988 |
| Grant date | Apr 10, 1990 |
| Priority date | — |
| Expiry date | Aug 25, 2008 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01J37/0201
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A process for producing supported metal catalysts having increased catalytic activity is provided. This process includes the steps of forming a high surface area porous support of a suitable porous material such as alumina or zirconia, dissolving a salt of a selected catalytic metal in an appropriate supercritical fluid solvent, contacting the porous support with the supercritical fluid solution of the catalytic metal salt to impregnate the porous support with the solution so that the catalytic metal salt may be adsorbed on the surfaces of the support, and removing the supercritical fluid solvent by reducing the pressure or increasing the temperature to change the supercritical fluid from the supercritical fluid phase to the gas phase, which may then be recycled for further use. The insoluble catalytic metal salt is deposited in the form of a film on the surfaces of the support. The catalytic metal salt-containing porous support may then be processed conventionally to produce a substantially pure, high activity supported metal catalyst.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.