Patent · US Expired

Mass spectrometer and method and improved ion transmission

US4963736A · kind A · utility

134Cited by
2References
24Claims
0Family size

Assignee

Inventors

Key dates

Filing dateNov 15, 1989
Grant dateOct 16, 1990
Priority date
Expiry dateNov 15, 2009

Classification

  • Technology area (CPC H)Electricity
  • CPC primaryH01J49/063
  • WIPO fieldElectrical machinery, apparatus, energy
  • WIPO sectorElectrical engineering

Abstract

In a mass spectrometer system, ions travel through an orifice in an inlet plate into a first vacuum chamber containing AC-only rods, and then through an orifice into a second vacuum chamber containing a standard quadrupole. The second vacuum chamber is held at low pressure, e.g. 0.02 millitorr or less, but the product of the pressure in the first chamber times the length of the AC-only rods is held above 2.25.times.10.sup.-2 torr cm, preferably between 6.times.10.sup.-2 and 15.times.10.sup.-2 torr cm, and the DC voltage between the inlet plate and the AC-only rods is kept low, e.g. between 1 and 30 volts, preferably between 1 and 10 volts. This produces a large enhancement in ion signal, with less focussing aberration and better sensitivity at high masses, and also allows the use of smaller, cheaper pumps so the system can be more easily transportable.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.