Patent · US Expired

Method of chromatographic separation

US5064539A · kind A · utility

42Cited by
13References
4Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 31, 1990
Grant dateNov 12, 1991
Priority date
Expiry dateOct 31, 2010

Classification

  • Technology area (CPC B)Performing Operations; Transporting
  • CPC primaryB01D15/1828
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

In a method using a chromatographic separation apparatus consisting of plurality of unit packed beds each having a supply inlet/extraction outlet, wherein the apparatus is effectively divided into four zones; an adsorption zone, a refining zone, a desorption zone, and a concentration zone. A supply and extraction step is performed in which all of the fluid flowing out of the adsorption zone is extracted through the nonadsorbate fluid extraction outlet, and then a recycle step, in which no fluid is supplied to or extracted from the bed, is performed to move the concentration distributions in the bed to a desired position. As a result, the method requires fewer unit beds, and enables extraction of components of higher purity.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.