Patent · US Expired

Oily, free-flowing, microcapsules

US5071706A · kind A · utility

64Cited by
7References
17Claims
0Family size

Assignee

Inventor

Key dates

Filing dateAug 31, 1989
Grant dateDec 10, 1991
Priority date
Expiry dateAug 31, 2009

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2984
  • WIPO fieldPharmaceuticals
  • WIPO sectorChemistry

Abstract

This disclosure is directed to the preparation of oily microcapsules which can be easily tray dried to a free flowing product without requiring special drying equipment. These microcapsules have a cell wall material having a first cell wall of gelatin/carboxymethylcellulose (CMC) which is prehardened (cross-linked) with a material selected from the group consisting of formaldehyde, glyoxal and glutaraldehyde to which there is grafted formaldehyde and urea. The predominant portion, viz., approximately 95% by wt. of these microcapsules have a particle size less than 1500 microns and more characteristically have a particle size ranging from about 100 to about 400 microns (microcapsular diameter). These microcapsules contain less than approximately 3 wt. % free oil and more characteristically less than about 1 wt. % free oil (non-microencapsulated oil) and have less free (unreacted) formaldehyde, which can be extracted with water, than do prior art microencapsulated oily materials. The microcapsules of this invention are granular and free-flowing when dried.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.