Patent · US Expired

Regeneration of zeolites used for purifying 1,1,1,2-tetrafluoroethane

US5087778A · kind A · utility

17Cited by
3References
20Claims
0Family size

Assignee

Inventor

Key dates

Filing dateApr 10, 1990
Grant dateFeb 11, 1992
Priority date
Expiry dateApr 10, 2010

Classification

  • Technology area (CPC B)Performing Operations; Transporting
  • CPC primaryB01J20/3491
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

1,1,1,2-Tetrafluoroethane (R134a) is purified to remove 50-10,000 wt. ppm of 2-chloro-1,1-difluoroethylene (R1122) by contacting with a zeolite or carbon molecular sieve having an average pore diameter of 3.8 to 4.8 Angstroms. The zeolite or carbon molecular sieve is regenerated by inert gas stripping residual R134a, followed by a regeneration at elevated temperatures using an inert gas. Regeneration of the zeolite or carbon molecular sieve is accomplished without the substantial reduction in capacity for impurities.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.