Separation of chloroform from a lower alcohol by extractive distillation
US5131985A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jun 3, 1991 |
| Grant date | Jul 21, 1992 |
| Priority date | — |
| Expiry date | Jun 3, 2011 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C17/38
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Chloroform cannot be completely separated from methanol, ethanol or isopropanol by conventional distillation or rectification because of the minimum boiling azeotrope between chloroform and the alcohols. Chloroform can be readily separated from methanol, ethanol or isopropanol by extractive distillation. Typical effective agents are: for methanol, isopropanol or 4-methyl-2-pentanone; for ethanol, n-butanol or isobutyl acetate; for isopropanol, butyl acetate or ethylene glycol ethyl ether.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.