Patent · US Expired

Laser ablation/ionizaton and mass spectrometric analysis of massive polymers

US5135870A · kind A · utility

86Cited by
5References
21Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJun 1, 1990
Grant dateAug 4, 1992
Priority date
Expiry dateJun 1, 2010

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T436/25875
  • WIPO fieldElectrical machinery, apparatus, energy
  • WIPO sectorElectrical engineering

Abstract

A sample containing one or more compounds of high molecular weight is analyzed by irradiating, with a pulsed laser in vacuum, a substrate coated with a thin frozen film of a solution containing the sample. The laser energy is absorbed at the surface of the substrate, rapidly heating the frozen film and ablating the solvent into a vapor plume which carries into the vapor phase entrained molecules of the sample. The vaporized molecules are ionized and accelerated into a mass spectrometer. Mass spectrometric determination of the masses of the ionized molecules of the sample allows the molecular components of the sample to be identified.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.