Preparation of 2-methylbenzoxazole
US5151523A · kind A · utility
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3Claims
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Key dates
| Filing date | Mar 11, 1991 |
| Grant date | Sep 29, 1992 |
| Priority date | — |
| Expiry date | Mar 11, 2011 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D263/56
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
A process for preparing 2-methylbenzoxazole by cyclizing acetamidophenol with the simultaneous elimination of the water of reaction. The process involves the drying and melting of the acetamidophenol, the cyclization of acetamidophenol to 2-methylbenzoxazole, and the removal of the water of reaction and the 2-methylbenzoxazole from the reaction mixture after the cyclization step by distillation. All the steps are carried out in a dryer.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.