Patent · US Expired

Epoxidate treatment

US5171868A · kind A · utility

12Cited by
7References
4Claims
0Family size

Assignee

Inventors

Key dates

Filing dateApr 15, 1992
Grant dateDec 15, 1992
Priority date
Expiry dateApr 15, 2012

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D301/32
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Caustic requirements are substantially reduced in the treatment of epoxidate from olefin/ethylbenzene hydroperoxide epoxidation by treating the epoxidate products with an aqueous stream comprised of alkali metal carbonate, separating a phenol-containing 1-phenyl ethanol fraction from the treated expodiate, separating phenol from the 1-phenyl ethanol fraction by treatment with basic anion exchange resin, regenerating the resin with aqueous alkali metal hydroxide, and converting alkali metal hydroxide from the resin regeneration to alkali metal carbonate for use in the epoxidate treatment.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.