Patent · US Expired

Microcrystalline alumina-based ceramic articles

US5185299A · kind A · utility

235Cited by
13References
20Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJul 9, 1990
Grant dateFeb 9, 1993
Priority date
Expiry dateJul 9, 2010

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01P2006/12
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

Microcrystalline alpha-alumina based ceramic articles comprising at least 60% alumina by weight, and 0.1-7.0 percent by weight iron equivalence in which substantially all the alumina is in the alpha phase having a uniform grain structure comprising alpha alumina crystallites with an average crystallite size less than 0.5 micrometer and a density greater than 90% theoretical are disclosed. Ceramic articles particularly useful as high modulus refractory fibers, among other shaped bodies such as beads, flakes, coatings, and shaped or randomly-shaped abrasive particles, are produced from a unique sol-gel process wherein hydroxy iron polymers are utilized to nucleate the alpha alumina transformation. An inherent advantage of the unique process disclosed is the resulting fine grained microstructure, and a surface roughness height of less than 100.0 nm, which is essential if a ceramic article such as an alpha alumina fiber is to have reasonable strength.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.