Patent · US Expired

Process for producing the precursor of a precipitated catalyst for the ammonia synthesis

US5221657A · kind A · utility

1Cited by
5References
20Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMay 29, 1991
Grant dateJun 22, 1993
Priority date
Expiry dateMay 29, 2011

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/52
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A process for producing the precursor of a precipitated catalyst for the sub.3 synthesis, based on Fe, Al, Co and K oxides, which comprises the steps of: PA0 (A) preparing an aqueous solution of water-soluble compounds of Fe, Al and Co--adding iron as a water-soluble ferrous salt of an organic acid--and causing, by addition of an alkaline precipitating solution, the co-precipitation of the corresponding (Fe, Al and Co) hydroxides, which still contain iron in the ferrous form; PA0 (B) oxidizing the hydroxide suspension prepared according to point (A) until divalent iron and trivalent iron are in a ratio to each other which ranges from 0.20 to 0.50; PA0 (C) operating an alkaline doping with a potassium compound and heating in an inert atmosphere up to above 850.degree. C.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.