Water-repellent metal oxide film coated on glass substrate and method of forming same
US5250322A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Dec 16, 1992 |
| Grant date | Oct 5, 1993 |
| Priority date | — |
| Expiry date | Dec 16, 2012 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10T428/31612
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
The disclosure relates to a metal oxide film formed on a glass substrate by the so-gel process with using a solution of a metal alkoxide. To afford water repellency to the oxide film, a fluoroalkylsilane is mixed with an alkoxysilane solution in the molar ratio of the alkoxysilane to the fluoroalkylsilane ranging from 1:10 to 10:1. Then, the mixed solution is diluted with a solvent such that the total concentration of the alkoxysilane and the fluoroalkylsilane is from 1 to 10 wt % in a diluted solution. Then, water in the amount of 100 mol % to 1000 mol % of the total amounts of the fluoroalkylsilane and the alkoxysilane is added to the diluted solution so as to partially hydrolyze the fluoroalkylsilane and the alkoxysilane, thereby forming a sol. Then, the sol is applied to the glass substrate, and the coated glass substrate is heated so as to form the metal oxide film thereon.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.