Process for the preparation of 2-nitro-3, 6-dichlorophenol
US5292966A · kind A · utility
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20Claims
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Key dates
| Filing date | Mar 16, 1993 |
| Grant date | Mar 8, 1994 |
| Priority date | — |
| Expiry date | Mar 16, 2013 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C201/08
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
2-Nitro-3,6-dichlorophenol is prepared by sulfonation of 2,5-dichlorophenol and subsequent nitration and desulfonation, in which the nitration is carried out by metering in a nitrating acid composed of 98 to 100% strength nitric acid and 96 to 100% strength sulfuric acid at temperatures from -15.degree. to 35.degree. C. and a metering time of at least 1 hour.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.