Patent · US Expired

Microdistillation method

US5304287A · kind A · utility

1Cited by
26References
15Claims
0Family size

Assignee

Inventor

Key dates

Filing dateFeb 7, 1991
Grant dateApr 19, 1994
Priority date
Expiry dateFeb 7, 2011

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T436/255
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

A microdistillation method for the quantitative steam distillation of cyanide, phenolic compounds, hydrogen fluoride, ammonia, sulfites and other volatile analyte compounds from samples of environmental waters and sludge for their subsequent analysis involves volatilizing the water in the sample tube of a microdistillation column. The pressure which develops due to the water vapor forces all volatile compounds from the water sample, including the water itself, through a hydrophobic membrane and into the collector tube of the microdistillation column. The volatile compounds and the water vapor condense in the cooler collector tube and are quantitatively trapped and retained over the membrane. Relatively small samples may be distilled.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.