Patent · US Expired

Process for the preparation of substituted pentaalkylchromenes

US5304663A · kind A · utility

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Key dates

Filing dateSep 15, 1993
Grant dateApr 19, 1994
Priority date
Expiry dateSep 15, 2013

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D311/58
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A novel process for the preparation of pentaalkylchromenes of the general formula: ##STR1## wherein R denotes a lower alkyl group having 1 to 4 C atoms and R.sub.1 denotes a phenyl group which is unsubstituted or substituted by a lower alkyl group having 1 to 4 C atoms, by halogen or by a nitro group, or an alkanoyl group having 1 to 4 C atoms. In the process, a trialkylhydroquinone is reacted with a halogenated butenol to give a substituted tetraalkyhydroquinone, which is oxidized. Then the halogen atom is substituted with a suitable nucleophile and the compound is finally cyclized to give the final product. The pentaalkylchromenes are suitable intermediates for the preparation of hypolipidaemic pharmaceuticals.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.