Patent · US Expired

Sulfate-free electroless copper plating baths

US5306336A · kind A · utility

10Cited by
11References
8Claims
0Family size

Assignee

Inventors

Key dates

Filing dateNov 20, 1992
Grant dateApr 26, 1994
Priority date
Expiry dateNov 20, 2012

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC23C18/405
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

Sulfate-free electroless copper baths comprising cupric ions, formaldehyde, formate ions, hydroxyl ions, a copper counterion, e g. preferably a monovalent anion such as acetate, nitrate or formate, and copper chelant such as an alkali metal salt of aminotris(methylenephosphonic acid), biscarboxymethylaspartic acid, ethylenediaminetetra(methylenephosphonic acid), diethylenetriaminepenta(methylenephosphonic acid), gluconic acid, 1-hydroxyethylidene-1,1-diphosphonic acid, mucic acid, D-saccharac acid, tartaric acid and N,N,N',N'-tetrakis(2-hydroxypropyl)ethylenediamine are amenable to the recovery of copper, e.g. from purge streams, using the methods and apparatus including solvent extraction, e.g. employing hydroxamic acid extractants, anion filtration, ion-exchange and chelant precipitation.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.