Azeotropic mixture of hydrogen fluoride and 1,1,1-trifluoro-2-chloroethane and process for purification of 1,1,1-trifluoro-2-chloroethane
US5324873A · kind A · utility
2Cited by
15References
12Claims
0Family size
Assignee
Inventors
Key dates
| Filing date | Feb 12, 1993 |
| Grant date | Jun 28, 1994 |
| Priority date | — |
| Expiry date | Feb 12, 2013 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C17/38
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Hydrogen fluoride and 1,1,1-trifluoro-2-chloroethane forms an azeotropic mixture. A mixture comprising hydrogen fluoride and 1,1,1-trifluoro-2-chloroethane is phase separated when it is cooled to a temperature below 7.degree. C. 1,1,1-Trifluoro-2-chloroethane is purified effectively from the mixture by cooling the mixture to form an upper liquid phase and a lower liquid phase and distilling the lower liquid phase so that the hydrogen fluoride is removed as an azeotropic distillate and 1,1,1-trifluoro-2-chloroethane substantially free from hydrogen fluoride is obtained as a bottom product.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.