Patent · US Expired

Water separation process

US5334784A · kind A · utility

10Cited by
5References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 9, 1992
Grant dateAug 2, 1994
Priority date
Expiry dateDec 9, 2012

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S502/514
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

Water present in a hot gaseous product stream from a reactor system A,B (FIG. 1 ) containing hydrogen fluoride is separated from the stream in order to eliminate a potentially corrosive combination of water and HF. The water is removed by contacting the gaseous product stream with liquid HF in a distillation column so as to obtain a bottoms product containing liquid HF and water and a top product containing dry HF and the product to be recovered. The invention encompasses the separation process, a vessel for carrying out the process (FIGS. 2 to 4), a control system for the liquid HF supply to the distillation column (FIGS. 5 and 6) and a recovery system for recovering HF employed during operation of the reactor system in different regimes employing HF as a fluorination agent, as a diluent during catalyst regeneration and/or catalyst prefluorination (FIG. 7 ).

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.