Process for producing acetaldehyde dimethylacetal
US5362918A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 23, 1993 |
| Grant date | Nov 8, 1994 |
| Priority date | — |
| Expiry date | Apr 23, 2013 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02P20/582
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A process for producing acetaldehyde dimethylacetal comprising reacting acetaldehyde and methanol in the presence of an acid catalyst is disclosed, in which the reaction is carried out in a part of a rectification tower while conducting rectification to withdraw the water by-produced from the bottom of the tower and to recover a distillate containing the acetaldehyde dimethylacetal produced from the top of the tower. The distillate is subjected to azeotropic distillation in the presence of n-hexane or cyclohexane to separate methanol as an azeotrope with n-hexane or cyclohexane and a small amount of the acetaldehyde dimethylacetal and to recover high purity acetaldehyde dimethylacetal as a bottom.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.