Patent · US Expired

Zero discharge process for manufacturing of phosphorous acid and hypophosphorous acid

US5368832A · kind A · utility

1Cited by
6References
8Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJun 7, 1991
Grant dateNov 29, 1994
Priority date
Expiry dateJun 7, 2011

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01B25/163
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

Disclosed is a method of making phosphorous acid or hypophosphorous acid by reacting hydrogen chloride with a sodium phosphite or a sodium hypophosphite, respectively, in the presence of water to precipitate sodium chloride crystals and form the acid. The acid is separated from the sodium chloride crystals and can be passed through an anion exchange column that is preferably loaded with phosphite or hypophosphite ions, respectively, to remove residual chloride ions.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.