Patent · US Expired

Heat- and chemical-resistant acrylic short fibers without spinning

US5401576A · kind A · utility

4Cited by
7References
5Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMay 20, 1993
Grant dateMar 28, 1995
Priority date
Expiry dateMay 20, 2013

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2913
  • WIPO fieldTextile and paper machines
  • WIPO sectorMechanical engineering

Abstract

A new, pulp-like, acrylic short fiber having excellent heat- and chemical-resistance is provided. The fiber has a thickness distribution of 0.1 .mu.m to 50 .mu.m, a length distribution of 1 mm to 20 mm, and a thermal transition temperature (Tg) of above 200.degree. C. The fiber is produced by heating a mixture of polyacrylonitrile and water of about 5% to 100% by weight to temperatures above hydration-melting temperature under seal to an amorphous melt; cooling the resulting amorphous melt to temperatures between the melting and the solidifying temperatures of the melt to form a supercooled melt; extruding the resulting supercooled melt to give extrudates; heat-stabilizing the resulting extrudates at temperatures between 180.degree. C. and 300.degree. C. for 1 minute to 4 hours after drying and drawing; and cutting and beating the resulting heat-stabilized extrudates into an appropriate size.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.