Patent · US Expired

Metal-interferon-alpha crystals

US5441734A · kind A · utility

52Cited by
5References
23Claims
0Family size

Assignee

Inventors

Key dates

Filing dateFeb 25, 1993
Grant dateAug 15, 1995
Priority date
Expiry dateFeb 25, 2013

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC30B29/58
  • WIPO fieldPharmaceuticals
  • WIPO sectorChemistry

Abstract

The present invention provides for crystalline zinc-interferon alfa-2 (IFN .alpha.-2) having a monoclinic morphology. The present invention further provides for crystalline cobalt-IFN .alpha.-2, crystalline calcium-IFN .alpha.-2, and crystalline IFN .alpha.-2 having a serum half-life of at least about 12 hours when injected into a primate. The present invention further provides for a method for producing a crystalline IFN .alpha.-2 comprising forming a soluble metal-IFN .alpha.-2 complex, and equilibrating the soluble metal-IFN .alpha.-2 complex in solution with an acetate salt of the metal under conditions that will cause the metal-IFN .alpha.-2 solution to become supersaturated and form crystalline metal-IFN .alpha.-2. The present invention also includes crystalline metal-alfa interferon having monoclinic, plate and needle morphologies.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.