Process for the electrochemical oxidation of arylketones
US5500099A · kind A · utility
1Cited by
1References
22Claims
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Assignee
Inventors
Key dates
| Filing date | May 9, 1995 |
| Grant date | Mar 19, 1996 |
| Priority date | — |
| Expiry date | May 9, 2015 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C45/54
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
The present invention provides a process for preparing arylglyoxals which comprise the steps of (a) electrochemically oxidizing an arylketone at a pH of less than about seven and at a temperature of from about -20.degree. C. to about 120.degree. C. in the presence of an electrolyte for a sufficient period of time to form an arylacetal, and (b) subjecting said acetal to hydrolysis for a sufficient period of time and under suitable temperature and pressure conditions to form said arylglyoxal.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.