Patent · US Expired

Toner aggregation processes using water insoluble transition metal containing powder

US5527658A · kind A · utility

266Cited by
13References
4Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 13, 1995
Grant dateJun 18, 1996
Priority date
Expiry dateMar 13, 2015

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG03G9/0815
  • WIPO fieldOptics
  • WIPO sectorInstruments

Abstract

A process for the preparation of toner comprising: PA1 (i) preparing a pigment dispersion comprised of pigment, an ionic surfactant, and optionally a charge control agent; PA1 (ii) shearing said pigment dispersion with a latex comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, and a nonionic surfactant; PA1 (iii) heating the above sheared blend of (ii) about below the glass transition temperature (Tg) of the resin, to form electrostatically bound toner size aggregates with a volume average diameter of from between about 2 and about 15 microns and with a narrow particle size distribution as reflected in the particle diameter GSD of between about 1.15 and about 1.30, followed by the addition of a water insoluble transition metal containing powder ionic surfactant in an amount of from between about 0.05 and about 5 weight percent based on the weight of the aggregates; and PA1 (iv) heating said bound aggregates about above the Tg of the resin to form toner.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.