Preparation of triphenylphosphine
US5527966A · kind A · utility
1Cited by
2References
9Claims
0Family size
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Key dates
| Filing date | Aug 3, 1994 |
| Grant date | Jun 18, 1996 |
| Priority date | — |
| Expiry date | Aug 3, 2014 |
Classification
- Technology area (CPC F)Mechanical Engineering; Lighting; Heating
- CPC primaryF16B2200/506
- WIPO fieldCivil engineering
- WIPO sectorOther fields
Abstract
Triphenylphosphine (TPP) is prepared by reacting triphenylphosphine dichloride (TPPCl.sub.2) with magnesium, aluminum and/or iron in the presence of an inert solvent, employing a TPPCl.sub.2 solution whose content of phosgene, chlorine, diphosgene, hydrogen chloride, thionyl chloride, sulfuryl chloride, phosphorus trichloride, phosphorus oxychloride and/or aliphatic halogen compounds (active chlorine compounds) totals less than 1000 ppm Cl.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.