Control of low inventory alkylation unit
US5583049A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 17, 1995 |
| Grant date | Dec 10, 1996 |
| Priority date | — |
| Expiry date | Apr 17, 2015 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10T436/21
- WIPO fieldMeasurement
- WIPO sectorInstruments
Abstract
A method and system for controlling an HF alkylation system comprising a reactor, a settler, an HF acid regenerator and a source of fresh HF acid wherein a stream of olefins and a stream of isobutanes are contacted in the reactor in the presence an HF acid catalyst. At least the reactor feed is sampled, and the sample is passed to an analyzer using an attenuated total reflectance cell. Signals are generated which are representative of infrared spectra of the samples in a range providing information on the amount of at least one of HF, water, ASO and sulfolane. These signals are simultaneously determined and generated because all absorb in the same spectral region. This aspect provides for viewing these distortions of the main HF absorption band to quantify these three components. The infrared spectra signals are compared with stored signals to generate control signals; and at least one of HF, water and sulfolane fed to the reactor feed is adjusted in response to the control signal.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.