Patent · US Expired

Rubber devulcanization process

US5602186A · kind A · utility

52Cited by
3References
26Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 27, 1995
Grant dateFeb 11, 1997
Priority date
Expiry dateOct 27, 2015

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02W30/62
  • WIPO fieldOther special machines
  • WIPO sectorMechanical engineering

Abstract

A process for devulcanizing a rubber vulcanizate by desulfurization involves suspending a rubber vulcanizate crumb in a solvent which preferably swells the rubber vulcanizate before or during the devulcanization reaction and adding an alkali metal, such as sodium, to the suspension. The alkali metal cleaves mono-, di- and polysulfidic cross-linkages in the rubber vulcanizate to liberate rubber polymer having a molecular weight substantially equal to that of the rubber polymer prior to vulcanization. Carbon black may also be recovered for re-use in accordance with the process of the present invention. Devulcanized rubber may be subjected to a re-vulcanization reaction without separation of rubber polymer from the solvent by addition of an appropriate curing mixture.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.