Process for production of multicyanate esters
US5648435A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Nov 17, 1995 |
| Grant date | Jul 15, 1997 |
| Priority date | — |
| Expiry date | Nov 17, 2015 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S210/908
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
A process of preparing multicyanate esters by: a) reacting an adduct of a tertiary amine and a phenol-formaldehyde oligomer or derivative thereof with cyanogen halide in a solvent reaction medium under conditions to form a reaction product stream containing at least one of the following compounds selected from the group consisting of tertiary amine-hydrohalide salt, solvent, and impurities, and, based upon the total weight of the reaction product stream excluding the weight of said tertiary amine-hydrohalide salt, from about 10 percent to about 40 percent of a multicyanate ester; b) recycling a portion of said reaction product stream into the mixture of step a; and c) separating and recovering said solvent and tertiary amine from said reaction product stream. The multicyanate ester products produced are useful as bonding agents in friction materials, molding materials, coatings, and adhesives.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.