Process for the detection of sulfur
US5661036A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | May 16, 1995 |
| Grant date | Aug 26, 1997 |
| Priority date | — |
| Expiry date | May 16, 2015 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10T436/188
- WIPO fieldMeasurement
- WIPO sectorInstruments
Abstract
A process and apparatus are disclosed for the detection and measurement of sulfur in both organic and inorganic sulfur-containing compounds. The process includes admixing a sample including a sulfur-containing compound with oxygen, and then exposing the mixture to a source of combustion causing heat in the presence of a combustion supporting reducing agent at a combustion site. The resulting gaseous combustion products are vacuum extracted from the combustion site, and then directed into a darkened low pressure chamber. The combustion products in the low pressure chamber are then contacted with ozone, with the result that the sulfur combustion products are converted to chemiluminescent sulfur dioxide. The emitted chemiluminescence is then detected, and may be measured to provide a quantitative indication of the amount of sulfur in the original sample. The preferred source of oxygen is air, the preferred form of combustion heat is a flame, and the preferred form of reducing agent is hydrogen gas.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.