Patent · US Expired

Synthesis of acetogenins

US5677467A · kind A · utility

4Cited by
1References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 3, 1996
Grant dateOct 14, 1997
Priority date
Expiry dateOct 3, 2016

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D307/58
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A method for the synthesis of bis-tetrahydrofuranyl annonaceous acetogenins, including the natural products and analogs thereof, is provided which proceeds by the Pd-mediated coupling of a bis-tetrahydrofuranyl-subunit comprising a terminal alkyne, with a (C4)-hydroxybutenolide subunit comprising a terminal vinyl iodide, followed by selective reduction of the resulting enyne.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.