Patent · US Expired

Process for preparing diphenylamines

US5679856A · kind A · utility

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3References
5Claims
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Assignee

Inventor

Key dates

Filing dateFeb 13, 1996
Grant dateOct 21, 1997
Priority date
Expiry dateFeb 13, 2016

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C213/02
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A process is described for preparing diphenylamines of the formula ##STR1## by oxybromination of a phenol ether compound using elemental bromine in the presence of hydrogen peroxide and of a catalyst to give a brominated phenol ether compound which is subsequently reacted with a formanilide compound to give the compound of the formula (1). The oxybromination reaction is a regioselective, environmentally friendly and cost-efffective method of preparing brominated aromatic compounds. The diphenylamines of the formula (1) are industrially useful intermediates for the production, for example of dyes, and in particular of color formers of the fluoran type for pressure- or heat-sensitive recording systems.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.