Patent · US Expired

Method for the preparation of dialkyl ethers

US5684213A · kind A · utility

37Cited by
22References
22Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 25, 1996
Grant dateNov 4, 1997
Priority date
Expiry dateMar 25, 2016

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/10
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A method for producing dialkyl ethers comprising feeding a stream containing a C.sub.1 to C.sub.4 alcohol to a distillation column reactor into a feed zone, contacting the stream with a fixed bed zeolite prepared as a distillation structure to form the corresponding dialkyl ether and water, and concurrently fractionating the ether product from the water and unreacted materials wherein the improvement is the addition of a small amount of hydrogen to the reaction zone to inhibit catalyst fouling and substantially increasing the catalyst life and activity.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.