2-alkylmercapto-4-(trifluoromethyl)benzoic esters and a process for their preparation
US5744021A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Dec 20, 1996 |
| Grant date | Apr 28, 1998 |
| Priority date | — |
| Expiry date | Dec 20, 2016 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C319/14
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
The invention relates to 2-alkylmercapto-4-(trifluoromethyl)benzoic esters of the formula (II), in which R.sup.1 and R.sup.2 are, independently of each other, (C.sub.1 -C.sub.6) alkyl, and a process for their preparation, which comprises reacting 3,4-dichlorobenzotrifluoride electrochemically at an anode with CO.sub.2 to give 2-chloro-4-(trifluoromethyl)-benzoate, converting it into the corresponding benzoic ester of the formula (I), and then reacting it with an alkylmercaptide R.sup.2 S.sup.e. ##STR1##
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.