Patent · US Expired

Preparation of alkyl cyanoacetates

US5756807A · kind A · utility

2Cited by
2References
8Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 21, 1996
Grant dateMay 26, 1998
Priority date
Expiry dateOct 21, 2016

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C253/30
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A process for preparing alkyl cyanoacetates of the general formula I ##STR1## where R is an n-valent aliphatic radical which has 6 to 20 carbon atoms and whose carbon framework can be interrupted by one to three oxygen atoms in ether functionality, and n is a number from 1 to 6, by reacting cyanoacetic acid in aqueous medium with an alcohol R(OH).sub.n, where the esterification is carried out in the presence of an inert entrainer and, during the reaction, water and entrainer are distilled out.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.