Patent · US Expired

Microcapsules and methods for making

US5827531A · kind A · utility

186Cited by
10References
84Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 2, 1994
Grant dateOct 27, 1998
Priority date
Expiry dateDec 2, 2014

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2989
  • WIPO fieldPharmaceuticals
  • WIPO sectorChemistry

Abstract

Methods of forming multi-lamellar microcapsules having alternating layers of hydrophilic and hydrophobic immiscible liquid phases have been developed using different polymer/solvent systems. The methods use liquid-liquid diffusion and simultaneous lateral phase separation, controlled by proper timed-sequence exposures of immiscible phases and low shear mixing, to form narrow size distributions of spherical, multilamellar microcapsules. The use of special formulations of solubilized drugs, surfactants, and polymeric co-surfactants in aqueous vehicles which are dispersed in hydrocarbon solvents containing small quantities of oil, low molecular weight co-surfactants and glycerides that are aqueous insoluble enables the formation of unique microcapsules which can carry large amounts of pharmaceuticals in both aqueous and non-aqueous solvent compartments. The liquid microcapsules are quickly formed in a single step and can include a polymeric outer "skin" which protects the microcapsules during physical manipulation or exposure to high shear forces. Water-in-oil and oil-in-water microcapsules have been formed both in 1.times.g and in microgravity, which contain several types of drugs co…

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.