Patent · US Expired

Preparation of nanocrystalline alloys by mechanical alloying carried out at elevated temperatures

US5837030A · kind A · utility

12Cited by
1References
13Claims
0Family size

Assignee

Inventors

Key dates

Filing dateNov 20, 1996
Grant dateNov 17, 1998
Priority date
Expiry dateNov 20, 2016

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S420/90
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

A process is described for preparing a nanocrystalline powder of an alloy of at least two metals by an intensive mechanical grinding step performed upon powders of the metals which make up the alloy. The grinding is performed at atmospheric pressure under an inert atmosphere, and is carried out at a temperature in the range of 100.degree.-400.degree. C. In this manner, one obtains crystallites of the alloy having a grain size lower than 100 nm by grinding for a period of time lower by about an order of magnitude than the time necessary to achieve this grain size by a similar grinding step carried out at ambient temperature.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.